2018年2月22日 星期四

Selective Catalytic Reduction (SCR) of NO by NH3 in a Fixed‐bed Reacto


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1.      Introduction         
Fossil fuels have been main sources for energy in terms of combustion, where chemical energy in fuels is converted into thermal and mechanical energies. When air reacts with fuels at high temperature, NOx representing NO, NO2, N2O, N2O5 and etc is unavoidable due to the reaction between oxygen and nitrogen in air [1, 2]. NOx is toxic as itself as well as a precursor of acid rain, so its regulation has been becoming more stringent all over the countries. There has been much interest in reducing NOx from engines in terms of fuel injection strategies [3], exhaust gas recirculation [4] and catalytic reactions [5], among which selective catalytic reduction (SCR) has been successfully applied in stationary applications such as boilers and power plants [6]. Although there are many reducing agents suggested, gaseous ammonia shows the best performance for this reaction [7]:        
4NH3 + 4NO + O2    4N2 + 6H2O                               (1.1)
Although the equation (1.1) is a major pathway for NO in the presence of O2, the equation (1.2) is also important when NO2 is high in the mixture of NO and NO2 [8].                                                 
4NH3 + 2NO + 2NO2   4N2 + 6H2O                             (1.2)
There have been many catalysts developed for the SCR reaction [9, 10], among which a V2O5/TiO2 catalyst has been widely used in commercial applications [10]. Although the equation (1.1) is an overall reaction for SCR, many elementary steps are involved during the reaction between NO and NH3 [11]. Since NO is reacted with NH3 on catalysts, its detailed reaction mechanism has been of great interest in order to develop kinetic models of SCR depending upon catalysts [12 – 14]. According to many studies, it is accepted that NO is reacted via the Langmuir‐Hinshelwood mechanism in V2O5‐WO3/TiO2 catalysts [13], where gaseous NO and NH3 are adsorbed on the catalysts and adsorbed NO and NH3 are reacted on the surface.           
There have been many researches for modeling of ammonia‐SCR systems [15 ‐ 19]. As evidenced by experiments, oxygen concentration in the exhaust gases is crucial for the SCR. Therefore, some kinetic models took into account the oxygen concentration [18, 19]. However, Chae et al. only considered NO and NH3 concentrations for their model although oxygen effect was already employed in their model [16]. Another important parameter in the SCR model is whether NH3 is oxidized by reacting oxygen as shown in the equation (1.3) [17, 18]. Since this reaction is active at high temperature over 400o C, it is observed that NO removal activity decreases over this temperature because NH3 which needs for NO reaction is converted into NO.                                                    
4NH3 + 5O2   4NO + 6H2O                                        (1.3)

In this study, the reaction between NO and NH3 was simulated in COMSOL using fundamental mass and momentum equations. The model was studied if it is appropriate to describe SCR reaction, which has been experimentally proven.


1.      Governing Equations
There are two governing equations employed in this model; one is a mass equation, and the other is a momentum equation. Although there is a heat evolved during the reaction of NO and NH3, an energy equation was not considered because it is very small due to small amounts of two reactants. The equation (2.1) indicates a mass equation in an advective flow.
where c is a concentration, D is a diffusion coefficient, R is a chemical reaction, and v is a velocity which is a vector form. Since the mass equation is assumed at a steady state, the 1st term is canceled out and finally the equation becomes the equation (2.2)                                      

For a momentum equation, the incompressible Navier‐Stokes equation in a laminar flow was employed as shown in the equation (2.3) and (2.4) 
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